Melting point Test
- Thread starter Lucky13
- Start date
BigRonWannabee
New member
Well first off, tell me what kind of powder its supposed to be, what it looks like (fluffly, crystals, fine powder, granules), the color (pure white, off white, caramel color, redish, brownish, be specific), if it has a strong odor, and any other physical attributes you can mention. Does it melt in your hands (in the baggie).
Take like 100mg and put it on some aluminum foil in a preheated oven and check that the temp is like 10 degrees COOLER than what its supposed to melt at. Then put it in and make sure it doesnt melt, check temp again. BTW do all the checking of melting with the oven OFF because it heat cycles.
Next bump up the temp 10 degrees and turn the oven off when it gets there (check temp) and put the sample back in. Wait a few minutes and check for meltage.
Do the same thing, bump up 10 degrees, check heat and put in sample with the oven off. Check for meltage.
If its MP is 300 degrees and it didnt melt at 290 or 300 but melted when you tried 310, its close enough and by referencing the physical propeties you can be pretty sure.
Take like 100mg and put it on some aluminum foil in a preheated oven and check that the temp is like 10 degrees COOLER than what its supposed to melt at. Then put it in and make sure it doesnt melt, check temp again. BTW do all the checking of melting with the oven OFF because it heat cycles.
Next bump up the temp 10 degrees and turn the oven off when it gets there (check temp) and put the sample back in. Wait a few minutes and check for meltage.
Do the same thing, bump up 10 degrees, check heat and put in sample with the oven off. Check for meltage.
If its MP is 300 degrees and it didnt melt at 290 or 300 but melted when you tried 310, its close enough and by referencing the physical propeties you can be pretty sure.
BigRonWannabee
New member
And yes you could do a double-boiler type setup and measure the exact liquid temp with an electronic thermometer when the sample melts but thats a pain. The oven way works fine. I havent tested a batch since my first one years ago.
BigRonWannabee
New member
You can buy electronic ones that have a probe you place in the oven, and you can leave it there with the wire coming out of the door (yes you can still close the oven its a tiny wire) and read the temp on a digital readout outside the oven. works well.
BigRonWannabee
New member
hahaha, copywrite date 6/21/2006 to DougoeFre5h.
Stamped, dated and approved!
Stamped, dated and approved!
BigRonWannabee
New member
lookin fantastic btw brotha man, excellent build. The quads and delts really pop, good fuckin work.